Chemical synthesis
Temperature-controlled reactions on jacketed vessels — heat, cool, hold and dose from a recipe beside the reactor.
rampsholdsdosing
Applications
Designed for laboratory chemistry.
FlexiFlow and FlexiConnect focus on jacketed glass reactor workflows for laboratory chemical synthesis and crystallisation. Support for individual instruments and vessels requires verification.
// CORE APPLICATIONSCHEMICAL SYNTHESIS · CRYSTALLISATION
These are intended workflow patterns, not claims of validated chemistry, verified compatibility or qualified processes. Equipment-specific integration and safety assessment are required.
Crystallisation
Cooling and antisolvent profiles with seeding and timed doses. Flagship example recipe below.
coolingseedingantisolvent
// FLAGSHIP EXAMPLECRYSTALLISATION RECIPE
Recipes in. Runs out.
One worked example: cooling + antisolvent crystallisation.
Cooling + antisolvent crystallisation
Adapted from Pickles et al., CrystEngComm 2024 · 7 steps · ~9 h · illustrative simulation
crystallisationtemperaturedosing
Swipe the chart to explore the full temperature profile →
- 1Ramp to 75 °C at 1 °C/min
- 2Hold 30 min
- 3Cool to 60 °C at 0.2 °C/min
- 4Seed and hold 30 min
- 5Dose 33.33 mL antisolvent over 45 min
- 6Hold 30 min
- 7Cool to 5 °C at 0.2 °C/min
Example recipe adapted from published research. Illustrative, not a validated procedure.
// STEPSFLAGSHIP PROFILE
Heat and hold
Ramp to 75 °C at 1 °C/min, then hold 30 min.
Cool, seed, hold
Cool to 60 °C at 0.2 °C/min. Seed. Hold 30 min.
Dose and finish
Dose 33.33 mL antisolvent over 45 min, hold 30 min, cool to 5 °C at 0.2 °C/min.
Design principles
Fail-safe behaviour in the design.
01
Sensor loss never counts as done.
A missing reading stops the step. It never completes it.
Under development02
A short dose blocks the next step.
No moving on until the intended amount is in.
Under development03
No automatic resume after power loss.
A person decides what happens next.
Under development04
Independent hardware safety stop.
In the design, even if software does not respond.
Under development